MD Sydul Islam

Analytical & Synthetic Chemist | R&D Scientist | Analytical Scientist | Process Development & Method Development | NMR | LC–MS | ICP-MS | HPLC | XRD | Six Sigma Green Belt

Detroit, Michigan, United States

About

Analytical and synthetic chemist with 7+ years of experience in inorganic, organometallic, coordination, and materials chemistry. Skilled in air/moisture-sensitive synthesis and analytical method development, with hands-on expertise across NMR, LC–MS, ICP–MS, HPLC, UV–Vis, FTIR, XRD, TGA, PL, and electrochemical techniques. Experienced in designing, optimizing, and characterizing macrocyclic ligands, lanthanide complexes, coordination polymers/MOFs, and nanomaterials. Strong foundation in structure elucidation, reaction optimization, and multi-technique analytical characterization. Industry-oriented skill set including DoE, method development & validation, process optimization, troubleshooting analytical instrumentation, GMP awareness, stability studies, and QMS-supported documentation. Proven ability to support formulation, analytical development, and process improvement initiatives across academic and pharmaceutical environments. Passionate about R&D, analytical science, materials chemistry, and process development roles in pharma, biotech, semiconductor, materials science, and chemical industries. Open to opportunities in Scientist, Analytical Development, R&D Chemist, and Process Engineer/MSAT roles.

Experience

  • Wayne State University ()
    • Graduate Research Assistant
      May 2022 - Present · 4 yrs 3 mos

      • Conduct advanced research in inorganic, synthetic, and materials chemistry, including design, optimization, and synthesis of macrocyclic ligands, lanthanide complexes, and MOF materials. • Apply analytical and structural characterization tools—NMR (1D/2D), LC–MS, GC-MS, ICP-MS, HPLC, UV–Vis, FTIR, XRD, TGA, PL, CV—to validate chemical structure, purity, and functional properties. • Develop and optimize experimental methodologies, improve process efficiency, and support data-driven decision-making using DoE and statistical approaches. • Troubleshoot analytical instrumentation and maintain high-quality documentation aligned with research and regulatory expectations. • Collaborate across multidisciplinary teams to execute R&D projects, interpret complex datasets, and deliver results under tight deadlines. • Mentor graduate and undergraduate researchers in lab techniques, method development, SOP compliance, and scientific communication.

    • Instrumentation Graduate Teaching Assistant
      Aug 2022 - May 2025 · 2 yrs 10 mos

      • Supported 5 undergraduate chemistry labs by maintaining, calibrating, and troubleshooting key analytical instruments, ensuring continuous and reliable lab operations. • Performed routine and advanced maintenance on analytical balances, pH meters, ATR-FTIR, benchtop NMR, GC, UV–Vis, titrators, rotary evaporators, and fluorimeters. • Streamlined laboratory workflows by optimizing calibration procedures, developing SOPs, and implementing instrument-readiness protocols. • Delivered hands-on training to 45+ Graduate Teaching Assistants on safe, accurate, and efficient use of analytical instrumentation. • Coordinated vendor communication, repair requests, and equipment diagnostics to minimize downtime and support lab quality standards.

    • Graduate Teaching Assistant
      Aug 2021 - Apr 2025 · 3 yrs 9 mos

      *Served across multiple non-consecutive terms (2021–2022, 2025) • Instructed undergraduate chemistry courses, including Chemistry Skills & Reasoning (CHM 1040) and General Chemistry I & II Labs (CHM 1130, CHM 1150), covering foundational theory, laboratory techniques, and basic analytical instrument use and maintenance. • Supported student learning through problem solving, mentoring, and dedicated office hours; evaluated assignments, lab reports, quizzes, and exams. • Conducted laboratory sessions, prepared materials, maintained safe and clean workspaces, and assisted with setup and organization of lab activities.

  • Analytical Development Executive at Eskayef Pharmaceuticals Limited
    Jan 2021 - Jun 2021 · 6 mos

    • Carried out both routine and non-routine analytical work for regulatory market. • Performed method development for Phytonadione injection (Vit. K1) product for the U.S. regulatory market. • Developed analytical testing methods of new product as well as conducted stability studies using HPLC, UV, and TLC thereof including proper retention of formulation and documentation.

  • Undergraduate and Graduate Research Student at Noakhali Science and Technology University
    Mar 2017 - Feb 2019 · 2 yrs

    • Synthesized and optimized novel Au@SiO2 nanocomposites by developing a fast and facile Ultrasonic method. • Utilized spectroscopic (UV−Vis, FTIR, XPS, and DLS) and other analytical techniques (XRD, SEM, and TEM) for structural confirmation and purity analysis.

  • Student Intern at Beximco Pharmaceuticals PLC
    Jun 2016 - Jun 2016 · 1 mo

    • Observed manufacturing operations across solid, liquid, and parenteral dosage processing units. • Gained exposure to equipment used in pharmaceutical production and packaging workflows. • Shadowed quality control activities and became familiar with analytical instruments used in QC labs. • Developed a foundational understanding of GMP expectations and pharmaceutical quality management systems.